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  • Mini Desktop X-Ray Diffractometer(XRD)
Mini Desktop X-Ray Diffractometer(XRD)

Mini Desktop X-Ray Diffractometer(XRD)

  • Model: DW-XRD-27Mini
  • Product description: Mini Desktop X-Ray Diffractometer(XRD)
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It is designed for commercial process and quality control. It is a concentration of advanced technology of XRD production, with multi-function and miniaturization. It can do qualitative analysis, quantitative analysis and crystal structure analysis on metal and nonmetal sample, especially for catalyst, titanium dioxide, cement and pharmacy industries.

 

Equipment Performance

●High frequency high voltage X-ray generator has greater stability, so it guarantees the repeatability of the data.

●Goniometer θs, θd arm adopts servo motor drive and optical encoder control technology, so the goniometer rotates more smoothly, the diffraction angle measuring is more accurate and the linearity is

better. Within the diffraction angle range, the diffraction linearity 0.02.

●The scattered ray protective device is safer and more reliable. When it is measuring samples, the protective door will be auto-locked to avoid the radiation to the people.

●DW-XRD-27mini XRD adopts the most advanced metal ceramic X-ray tube, it has long service life (3000 hours); the automatic 6-sample changer can improve the sample measuring speed and convenient for the operator.

●The compact structure can installed onto the platform without special laboratory environment. It is easy for operation and maintenance.

 

Application

ADW-XRD-27mini XRD can do qualitative and quantitative analysis on polycrystalline material. During qualitative analysis, it will indentify the unknown structure by comparing the measuring data with known phase data base. During quantitative analysis, it can describe the characteristics of the solid mixture, so that to confirm relative content of the crystalline compounds or un-crystallized phase.
Technical parameters

Service rating

Tube voltage, tube current

600W(40kV,15mA) or 1200W(40kV,30mA),Stability:0.005%

X-ray tube

Metal-ceramic X-ray tube, Cu target, Power 2.4kW, Focus size:

1 x 10 mmAir cooling or water coolingwater flow rate 1L/min

Goniometer

θs-θd , diffraction radius 150mm

Measuring method

Continuous, stepping, Omg

Angular measurement range

Druing leakage time, θs/θd is -3°150°.

Minimum step width

0.0001°

Angular reproducibility

0.0001°

Drive mode

servo motor drive + optical encoder control technology

Angle Positioning speed

1500°/min

Counter

Closed Proportional detector or High speed one-dimensional semiconductor counter

Energy spectrum resolution

25%

Max. linear counting rate

≥5×105cpsProportional,≥1×107cpsOne-dimensional

semiconductor

Computer

Dell laptop

 

 

 

 

 

Software

 

 

Controlling software

Windows 7 operating system; control the tube voltage, tube current, shutter of the X-ray generator and do aging training automatically; Control the goniometer continuous or stepping scanning and diffraction data collection; do routine processing: automatic

peak-seeking, manual peaking-seeking, integrated intensity, peak height, core, background deduction, smoothness, Peak shape amplification and spectrogram comparation, etc.

 

 

Data processing software

Qualitative and quantitative analysis of material phases , Kα1 ,α2 peeling, Full spectrum fitting, peak fitting, half-width and grain size calculation, crystal cell measuring, second kind stress calculation, diffraction line indexation, multiple plotting, 3D plotting, diffraction data calibration, background subtraction, quantitative analysis without standards, full spectral image fitting (WPF), XRD diffraction image simulation, etc.

Scattered radiation protection

Lead+ lead glass protection, shutter windows and protective guard linkage, the scattered radiation dose not exceeding 1μSv/h.

Instrument Comprehensive regulation

≤1‰

Sample quantity of one-time loading

Auto sample changer, 6 samples can be put one time.

Overall dimension

600×410×670w×d×hmm


DW-XRD-27 MINI Desktop XRD Configuration Table

Name

Components

Unit

Qt

y Remark

 

X-ray

high-voltage generator

XRD40*600 X-ray generator

set

1

high-frequency high-voltage

X27.06 high-voltage cable75kVP

piece

1

Length2.0 meter

3311 pipe sleeve (including automatic optical shutter)

set

1

 

X25.02 stage(Metal shell)

set

1

Lead+ lead glass protection

DS2910/24 Metal ceramic insulation X-ray tube

piece

1

Cu target, 2.4kW

 

 

Angle measurement system

DG-3511 goniometer

set

1

θ-θ structure

Slit and powder sample holder

set

1

One set for each

Through-hole sample plate

piece

5

Aluminium matrix

Blind-hole sample plate

piece

10

Glass matrix

Filter

piece

1

Match with target material

Slit plate and lighting system adjustment accessories

set

1

 

Recording and controlling system

Closed proportional counter

set

1

Including 1 piece of connecting cable

Recording and controlling unit

set

1

 

Motor and communication cable

piece

1

2 motor cables, 1 communication cable

Power supply unit

set

1

 

 

PC system

Dell laptop; I3 processor; RAM:4G; Hard drive: 500G;

set

1

DELL

A4 laser printer

set

1

 

 

System Control and Applicable Software

AL Series Diffractometer Control Program Software

set

1

Windows OS

Diffraction data processing software

set

1

 

Diffraction data card base

set

1

2009 version59

Crystal Structure Data Base

set

1

2010 version

Technical documents

AL series XRD user manual

copy

1

 

Data Process and Applicable Software User Manual

copy

1

 

Accessory

DCX-6 sample changer

set

1

 

Graphite monochromator

set

1

Reflectivity28%

 

Spare parts

Fuses 11.522.533+A

Piece

10

10 pieces for each

Tools

set

1

 

Agate Mortar ф100mm

set

1

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